Start with three measurements: purity (HPLC), identity (mass spectrometry) and net content. Together they catch the wrong molecule and the underfilled vial, which purity alone can't. The others answer different questions:
Which of these your sample needs depends on the compound, how you'll use it and for how long. Plan a peptide test asks eight questions and returns the tests, the labs that run them and what they cost. How to test your peptides covers sending a sample; a base panel costs $150–$325 (verified October 2026), and the page lists what's in it.